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1、Designation:D7234?12StardTestMethodfPullOffAdhesionStrengthofCoatingsonConcreteUsingPtablePullOffAdhesionTesters1ThisstardisissuedunderthefixeddesignationD7234thenumberimmediatelyfollowingthedesignationindicatestheyearof
2、iginaladoptioninthecaseofrevisiontheyearoflastrevision.Anumberinparenthesesindicatestheyearoflastreapproval.Asuperepsilon()indicatesaneditialchangesincethelastrevisionreapproval.1.Scope1.1Thistestmethodcoversproceduresfe
3、valuatingthepulloffadhesionstrengthofacoatingonconcrete.Thetestdeterminesthegreatestperpendicularfce(intension)thatasurfaceareacanbearbefeaplugofmaterialisdetached.Failurewilloccuralongtheweakestplanewithinthesystemcompr
4、isedofthetestfixtureadhesivecoatingsystemsubstratewillbeexposedbythefracturesurface.1.2Thistestmethodusesaclassofapparatusknownasptablepulloffadhesiontesters.2Theyarecapableofapplyingaconcentricloadcounterloadtoasinglesu
5、rfacesothatcoatingscanbetestedeventhoughonlyonesideisaccessible.Measurementsarelimitedbythestrengthofadhesionbondsbetweentheloadingfixturecoatingsystemthesubstratethecohesivestrengthsoftheadhesivecoatinglayerssubstrate.1
6、.3Pulloffadhesionstrengthmeasurementsdependuponbothmaterialinstrumentalparameters.Therearedifferentinstrumentsusedthatcomplywiththistestmethod.Thespecificinstrumentusedshouldbeidentifiedwhenreptingresults.Thistestisdestr
7、uctivespotrepairsmaybenecessary.1.4ThevaluesstatedinSIunitsaretoberegardedasthestard.Thevaluesgiveninparenthesesarefinfmationonly.1.5Thisstarddoesnotpurpttoaddressallofthesafetyconcernsifanyassociatedwithitsuse.Itisthere
8、sponsibilityoftheuserofthisstardtoestablishappropriatesafetyhealthpracticesdeterminetheapplicabilityofregulatylimitationspritouse.2.ReferencedDocuments2.1ASTMStards:3C1583TestMethodfTensileStrengthofConcreteSurfacestheBo
9、ndStrengthTensileStrengthofConcreteRepairOverlayMaterialsbyDirectTension(PulloffMethod)D16TerminologyfPaintRelatedCoatingsMaterialsApplicationsD2651GuidefPreparationofMetalSurfacesfAdhesiveBondingD3933GuidefPreparationof
10、AluminumSurfacesfStructuralAdhesivesBonding(PhosphicAcidAnodizing)D4541TestMethodfPullOffStrengthofCoatingsUsingPtableAdhesionTestersE177PracticefUseoftheTermsPrecisionBiasinASTMTestMethodsE178PracticefDealingWithOutlyin
11、gObservationsE691PracticefConductinganInterlabatyStudytoDeterminethePrecisionofaTestMethod3.Terminology3.1ThetermsdefinitionsinTerminologyD16applytothistestmethod.3.2Definitions:3.2.1adhesiven—(withrespecttothistestmetho
12、d)adhesivereferstothematerialthatbondsthebottomoftheloadingfixturetothetopsurfaceofthecoatingtobetested.3.2.2loadingfixturen—(alsoreferredtoasdolliesstuds)ametalstructurethatisflatononeendfbondingtothecoatingsurfaceshape
13、dontheotherendfattachmenttotheadhesiontesterisusedtodeterminethepulloffadhesionstrengthofcoatings.3.2.3ptablepulloffadhesiontestersn—instrumentsthatarecapableofapplyingaconcentricloadcounterloadto1Thistestmethodisunderth
14、ejurisdictionofASTMCommitteeD01onPaintRelatedCoatingsMaterialsApplicationsisthedirectresponsibilityofSubcommitteeD01.46onIndustrialProtectiveCoatings.CurrenteditionapprovedJuly12012.PublishedOctober2012.iginallyapprovedi
15、n2005.Lastpreviouseditionapprovedin2005asD7234–05.DOI:10.1520D723412.2Thetermadhesiontestermaybesomewhatofamisnomerbutitsadoptionbytwomanufacturersatleasttwopatentsindicatescontinuedusage.3FreferencedASTMstardsvisittheAS
16、TMwebsitewww.astm.gcontactASTMCustomerServiceat.FAnnualBookofASTMStardsvolumeinfmationrefertothestard’sDocumentSummarypageontheASTMwebsite.Copyright?ASTMInternational100BarrHarbDrivePOBoxC700WestConshohockenPA194282959.U
17、nitedStates1fixture.Atleastthreereplicationsarerequiredindertostatisticallyacterizethetestarea.7.1.2Theedtestareasmustalsohaveenoughperpendicularradialclearancetoaccommodatetheapparatusbeflatenoughtopermitalignment.Itsho
18、uldbenotedthatmeasurementsclosetoanedgemaynotberepresentativeofthecoatingasawhole.7.2Scingthecoatingdowntothesurfaceofthesubstrateisrequiredfallcoatingsthickerthan0.5mm(20mils)fallreinfcedelastomericcoatings.Whilescingis
19、recommendedfcoatingsthinnerthan0.5mm(20mils)thetestmaybeperfmedwithoutscingbuttheresultsshouldnotethisexception.Scingshallbeperfmedinamannerthatensuresthecutismadenmaltothecoatingsurfaceinamannerthatdoesnottwisttquethete
20、stareaminimizesheatgeneratededgedamagemicrocrackstothecoatingtheconcretesubstrate.Fthickcoatingsitisrecommendedtocoolthecoatingsubstrateduringthecuttingprocesswithwaterlubrication.Whenusingaroundloadingfixturescingisperf
21、medbefetheloadingfixtureisattached(seeFig.1).Whenusingsquarerectangularloadingfixturesscingistypicallyperfmedaftertheloadingfixtureisattached(seeFig.2).7.3Cleanthesurfacesinamannerthatwillnotaffectintegrityofthecoatingle
22、avearesidue.Cleantheloadingfixturesurfaceasindicatedbytheapparatusmanufacturer.FailuresatthefixtureadhesiveinterfacecanoftenbeavoidedbytreatingthefixturesurfacesinaccdancewithanappropriateASTMstardpracticefpreparingmetal
23、surfacesfadhesivebonding.Fingerprintsmoistureoxidestendtobetheprimarycontaminants.NOTE1—GuidesD2651D3933aretypicalofwellprovenmethodsfimprovingadhesivebondstrengthstometalsurfaces.7.4Preparetheadhesiveinaccdancewiththead
24、hesivemanufacturer’srecommendations.Applytheadhesivetothefixturethesurfacetobetestedbothusingamethodrecommendedbytheadhesivemanufacturer.Becertaintoapplytheadhesiveacrosstheentiresurface.Positionfixtureonthesurfacetobete
25、stedcentereddirectlyoverthescedsectionwiththefixtureoutersideslinedupwiththeinsidecircumferenceofthescedsection.Carefullyremovetheexcessadhesivefromaroundthefixture.(Warning—Movementespeciallytwistingcancausetinybubblest
26、ocoalesceintolargeholidaysthatconstitutestressdiscontinuitiesduringtesting.)NOTE2—Addingabout1percentof#5glassbeadstotheadhesiveassistsinevenalignmentofthetestfixturetothesurface.7.5Basedontheadhesivemanufacturer’srecomm
27、endationstheanticipatedenvironmentalconditionsallowenoughtimeftheadhesivetosetupreachtherecommendedcure.Duringtheadhesivesetearlycurestageaconstantcontactpressureshouldbemaintainedonthefixture.Mechanicalclampingsystemswk
28、wellbutsystemsrelyingontacksuchasmaskingtapeshouldbeusedwithcaretoensurethattheydonotrelaxwithtimeallowairtointrudebetweenthefixturethetestarea.FIG.1ScingAroundtheLoadingFixturePritoAttachmentoftheFixture(RoundLoadingFix
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