版權(quán)說(shuō)明：本文檔由用戶提供并上傳，收益歸屬內(nèi)容提供方，若內(nèi)容存在侵權(quán)，請(qǐng)進(jìn)行舉報(bào)或認(rèn)領(lǐng)
文檔簡(jiǎn)介
1、YangtzeRiverPharmaceuticalGroup揚(yáng)子江藥業(yè)集團(tuán)有限公司揚(yáng)子江藥業(yè)集團(tuán)有限公司1ReptProject:PolygoniientalisfructusCustomernameaddress:YuanYeNKITCMProjectobjective:EvaluateTLCmethodsfPolygoniientalisfructusDate:8thFebruary2011Labaty:NKITCMApprove
2、dby:Dr.LuZhengDr.TingXianAimEstablishmentofTLCmethodsfdeterminationofTaxifolininPolygoniientalisfructus1.GeneralexperimentaldetailsTable1SamplesstardsidentificationSamplenumberSampledeionSourceSupplierBatchS001Polygoniie
3、ntalisfructusAnguoginsengantlerlimitedcompanyAnguocityHebeiprovinceL201010S002PolygoniientalisfructusAnguoginsengantlerlimitedcompanyAnguocityHebeiprovinceJ201010S003PolygoniientalisfructusBeijingTongrentangpharmacyBeiji
4、ng20101112S004PolygoniientalisfructusBeijingYongantangpharmacyBeijing20101118S005PolygoniientalisfructusLotuspondTCMwholesalemarketChengducitySichuanprovince201011WUHongweiS006PolygoniientalisfructusZhongyiyuanpharmacySh
5、enyangcityLiaoningprovince101201S007PolygoniientalisfructusTaizhouGaogangTCMCo.LTDTaizhouCityJiangsuprovince030111S008PolygoniientalisfructusJilincityJilinprovince20101121S009PolygoniientalisfructusChinaNepstarChinDrugst
6、reLTDSipingcityJilinprovince091227S010PolygoniientalisNtheastpharmacyShenyangcityLiaoning201011YangtzeRiverPharmaceuticalGroup揚(yáng)子江藥業(yè)集團(tuán)有限公司揚(yáng)子江藥業(yè)集團(tuán)有限公司3Testsolution:Heat2gofthepowdereddrugin5mlofmethanolRunderarefluxcondens
7、erf10min.Coolthenfiltered.Usethefiltrateasthetestsolution.Referencesolution:Dissolve1mgoftaxifolinRin2mlofmethanolR.Dissolve1mgofkaempferolRin10mlofmethanolR.3.Results(plates)ApplicationInstrument:DrummondscientificCOUSA
8、Blength:8mmDistancebetweentracks:7mmApplicationposition:X:20mmY:10mmChromatographyPlate:HPTLCglass20X10cmSi60Chamber:ADC2Plateconditioning:at50%huitySaturation:60minwithfilterpaperDevelopingdistancefromapplicationpositio
9、nloweredge:80mm.Developingsolvent:TrichlomethaneRAcetoneRGlacialaceticacidRanhydrousFmicacidR(20:1:2:2VVVV).Platedrying:10min105℃.Detection:spraythewarmplatewitha10gLsolutionofdiphenylbicacidaminoethylofesterRinmethanolR
10、thenwiththesamevolumeofa50gLsolutionofmacrogol400RinmethanolRallowdryinginairfabout30minevaluatingunderUV365nm.TopoftheplateAgreenzoneAredzoneApalebluefluescentzoneAdiffusegreenfluescentzoneAbluefluescentzoneAgreenfluesc
溫馨提示
- 1. 本站所有資源如無(wú)特殊說(shuō)明，都需要本地電腦安裝OFFICE2007和PDF閱讀器。圖紙軟件為CAD,CAXA,PROE,UG,SolidWorks等.壓縮文件請(qǐng)下載最新的WinRAR軟件解壓。
- 2. 本站的文檔不包含任何第三方提供的附件圖紙等，如果需要附件，請(qǐng)聯(lián)系上傳者。文件的所有權(quán)益歸上傳用戶所有。
- 3. 本站RAR壓縮包中若帶圖紙，網(wǎng)頁(yè)內(nèi)容里面會(huì)有圖紙預(yù)覽，若沒(méi)有圖紙預(yù)覽就沒(méi)有圖紙。
- 4. 未經(jīng)權(quán)益所有人同意不得將文件中的內(nèi)容挪作商業(yè)或盈利用途。
- 5. 眾賞文庫(kù)僅提供信息存儲(chǔ)空間，僅對(duì)用戶上傳內(nèi)容的表現(xiàn)方式做保護(hù)處理，對(duì)用戶上傳分享的文檔內(nèi)容本身不做任何修改或編輯，并不能對(duì)任何下載內(nèi)容負(fù)責(zé)。
- 6. 下載文件中如有侵權(quán)或不適當(dāng)內(nèi)容，請(qǐng)與我們聯(lián)系，我們立即糾正。
- 7. 本站不保證下載資源的準(zhǔn)確性、安全性和完整性, 同時(shí)也不承擔(dān)用戶因使用這些下載資源對(duì)自己和他人造成任何形式的傷害或損失。
最新文檔
- 柱層析和tlc
- tlc認(rèn)證收費(fèi)標(biāo)準(zhǔn)
- learning methods
- tlc板技術(shù)經(jīng)驗(yàn)交流
- optimization on the extraction of polysaccharides from fructus corni using uniform design
- tlc各種顯色劑及其配制方法
- tlc中展開(kāi)劑的選擇
- tlc549中文介紹
- statistical methods in epidemiologic research
- 薄層色譜(tlc)的使用指南
- my methods to learn english
- variational methods (michael struwe)
- induction motor starting methods and issues
- programmed necrosis methods and protocols 2018
- first-order methods in optimization
- control systems and mathematical methods in economics
- 2018版-myogenesis methods and protocols
- 薄層層析tlc通用顯色劑
- 2016版-the nucleolus methods and protocols
- IC-TLC、RV-TLC和BMI在綜合評(píng)估慢性阻塞性肺疾病中的價(jià)值.pdf
評(píng)論
0/150
提交評(píng)論