不對(duì)稱有機(jī)催化反應(yīng)金雞納生物堿衍生物催化不對(duì)稱“中斷的”feistb233;nary反應(yīng)_第1頁(yè)
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1、第四軍醫(yī)大學(xué)博士學(xué)位論文 0目 錄 縮略語(yǔ)表································

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7、;·····3 英文摘要······························

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10、;······7 第一章 文獻(xiàn)綜述 ····························

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12、183;····························11 第二章 正文 ······&#

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15、3;······················37 2.1 金雞納生物堿酯類衍生物的合成及其在不對(duì)稱 IFB 反應(yīng)中的應(yīng)用····37 2.2 金雞納生物堿醚類衍生物的合成及其在

16、不對(duì)稱 IFB 反應(yīng)中的應(yīng)用····49 2.3 金雞納生物堿胺類衍生物的合成及其在不對(duì)稱 IFB 反應(yīng)中的應(yīng)用····56 2.4 金雞納生物堿硫脲類衍生物的合成及其在不對(duì)稱 IFB 反應(yīng)中的應(yīng)用 64 2.5 金雞納生物堿衍生物催化不對(duì)稱 IFB 反應(yīng)的機(jī)理 ········

17、·······················71 第三章 實(shí)驗(yàn)部分 ···········

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20、·········73 全文總結(jié)··························

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23、;······101 參考文獻(xiàn)·····························&

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29、3;···························120 個(gè)人簡(jiǎn)歷和研究成果 ·······

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32、183;·····136 致謝······························

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35、183;··········138 第四軍醫(yī)大學(xué)博士學(xué)位論文 2PMP p-methoxypheyl 對(duì)甲氧基苯基 pKa 電離平衡常數(shù)負(fù)對(duì)數(shù) PPA polyphosphoric acid 多聚磷酸 PS Proton Sponge 質(zhì)子海綿 SN2 nucleophilic substitution reaction

36、雙分子親核加成反應(yīng) QN quinine 奎寧 QD quinidine 奎尼定 THF tetrahydrofuran 四氫呋喃 TLC thin layer chromatography 薄層色譜法 Ts 4-toluene sulfonyl 對(duì)甲苯磺酰基 TsOH 4-toluenesulfonic acid 對(duì)甲基苯磺酸 % ee percent enantiomeric excess 百分對(duì)映體過量

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