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1、貴 州 大 學2009 2009 2009 2009 屆碩士研究生學位論文不對稱 1,5-二芳基-1,4-戊二烯-3-酮類化合物的合成及生物活性研究學科專業(yè)： 農(nóng) 藥 學研究方向： 新農(nóng)藥與新藥物設(shè)計和合成導 師： 胡 德 禹 ( 研 究 員)研 究 生： 于 大 偉中國·貴州·貴陽2009 年 5 月分 類 號 ： O 6 2 3 . 5 2 2論文編號： 2006140996密 級：3.3 3.3 3.3 3.3

2、 目標化合物的合成 目標化合物的合成·································

3、3;····································&#

4、183;·············273.3.1 不對稱 1,5-二取代芳基-1,4-戊二烯-3-酮類化合物(I I I IA A A A)的合成..................................... 273.3.2 不對稱 1,5-二取代芳基-1,4-戊二烯-3-酮類化合物(I I I

5、IB B B B)的合成......................................333.3.3 乙基苯基碳酸酯類化合物(II II II II)的合成..............................................................................343. 3. 3. 3.4 4 4 4 目標化合物的生物活性測試方法 目標化合物的生物活性測試方法·&

6、#183;····································

7、;····························363.4.1 目標化合物抑菌活性測試方法..............................

8、..........................................................363.4.2 目標化合物體外抗腫瘤活性測試方法.............................................................................36第四章 結(jié)果與討論 結(jié)果與討論·······&#

9、183;····································

10、····································

11、3;··············384.1 4.1 4.1 4.1 目標化合物合成方法研究 目標化合物合成方法研究···············

12、83;····································&

13、#183;······················384.1.1 目標化合物 I I I I 的合成方法討論......................................................

14、.................................. 384.1.2 目標化合物 II II II II 的合成方法討論.......................................................................................394.2 4.2 4.2 4.2 目標化合物的波譜解析 目標化合物的波譜解析····&#

15、183;····································

16、····································

17、3;404.2.1 目標化合物 I I I I 的譜圖解析................................................................................................ 404.2.2 目標化合物 II II II II 的譜圖解析...............................................................

18、................................414.3 4.3 4.3 4.3 目標化合物的生物活性測定 目標化合物的生物活性測定························&

19、#183;····································

20、;···········424.3.1 目標化合物抑菌活性測試結(jié)果........................................................................................424.3.2 目標化合物體外抗腫瘤活性測試結(jié)果....................

21、.........................................................43第五章 結(jié)論及展望 結(jié)論及展望························&#

22、183;····································

23、··································455.1 5.1 5.1 5.

24、1 結(jié)論 結(jié)論···································

25、83;····································&

26、#183;·································455.2 5.2 5.2 5.2

27、 創(chuàng)新點 創(chuàng)新點···································&#

28、183;····································

29、································455.3 5.3 5.3 5.3 不足與 不足與展望

30、展望····································&#

31、183;····································

32、························45致 謝············

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34、83;····································&

35、#183;························· 46參考文獻 參考文獻·········

36、;····································

37、83;····································&

38、#183;························· 47附 錄··········

39、;····································

40、83;····································&

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